Distillation is the basic and oldest chemical separation process used in the chemical industries and petroleum refining.
Let's recognize the difference between Packed and Plate columns in industry and the comparison of their usage!
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Added: Dec 25, 2019
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Tray vs. Packed Column
For Chemical Engineering Applications
= Plate columns can handle wide range of gas and liquid flow rates.
= Plate column provide stage controlled contact.
= Plate column operation is considerably smooth.
Plate efficiency can be predicted more accurately
When the liquid cause fouling or deposition of solids, even though the tray
is blocked up, it is easier to clean it.
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Plate Column
Introduction
Ca Ta
Cul
= Plate column is composed of several equilibrium stages.
= Every Equilibrium Stage has its own VLE (vapour liquid equilibrium)
different
VLE in Equilibrium stages are related to previous equilibrium stage
VLE and affect the next one.
= Equilibrium Stage is called tray.
= Tray has different designs (bubble cap - valve - sieve)
Tray Downcomer
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Plate Column Anatomy
Basic Components of Tray Column
= Inlets:
V The feed inlets are located between the rectifying and stripping sections.
Y Distillation columns can have three or more feed lines.
= Dutlets:
V The overhead outlet is the vapor exit point from the distillation column to pass into the condenser.
Y” The bottoms outlet is used to remove residue from the distillation column and to feed the reboiler.
v The side stream outlet is used to remove side product in multicomponent distillation processes
= Feed Tray: The location of the feed tray is determined by the ratio of stages above and below the inlet feed
line
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Plate Column Anatomy de
Basic Components of Tray Column E I~ i.
" Rectifying Section: t — y | y
Y is located above the feed tray. Rs = an Baa
y” has a higher concentration of light components than the |
stripping section t
Stripping ection is
= Stripping Section | e
v is located below the feed tray. |
v has a higher concentration of light components than the oy
stripping section.
Y” Temperatures in the stripping section are usually much higher than in the rectifying section
Bottoms Product
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Tray vs. Packed Column for Chemical Engineering Applications
Bottom System
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Plate Column Anatomy
There are three types of trays used in
distillation towers:
+ Bubble Cap Tray
+ Valve Tray
+ Sieve Tray
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Plate Column Anatomy
Types of Trays
Low Vapour ‘Normal Vapour Hight Vapour sebetray
Bubble Cap Tray Valve Tray Sieve \ Perforated Tray
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Plate Column Anatomy
Types of Trays
a) Bubble Cap Tray
q Wer
L-
= Bubble-cap trays are used commonly in the distillation process.
= Aweir on the tray maintains a liquid level over the caps.
= This vapor comes into direct contact with the liquid on the tray
and transfers some heat energy.
= The liquid condenses the heavier components of the vapor,
whereas the lighter components move up the tower.
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Plate Column Anatomy
Types of Trays
b) Valve Tray
= Valve trays have simple, movable plates.
= Plate movement depends on process flow.
= This type of tray is more efficient over a wider range of flow rates
than the sieve tray
‘Normal Vapour Hight Vapour
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Plate Column Anatomy
Types of Trays
c) Sieve tray
Sieve trays are the simplest type of tray.
A sieve tray is essentially a metal plate with small holes in it.
Vapor comes through the holes, it moves too fast to be stapped by
the liquid level on the tray, but it does slow down significantly as it
passes through the liquid.
The holes range from | inch to 1/8th inch in diameter.
Pressure drop through a large number of small holes is greater
than the drop through fewer large holes
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Plate Column Anatomy
Tray Classification according to Pass NO.
Tray Pass
= The more paths for liquid flow, the higher the liquid handling capacity
= Liquid flow paths change pressure balance, multiple flow paths can increase vapor capacity as well
= 1,2 4 paths common
= 3used occasionally
= 5+ not common
= The more passes, the larger the tower minimum diameter
= The active area should be a minimum width to allow for manways
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Plate Column Anatomy
Tray Classification according to Pass NO.
Ea Eb En EX
TWO PASS THREE PASS FOUR PASS FIVE PASS
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Plate Column Anatomy
Basic Components of Tray Column
= Weir:
The function of a weir is to maintain a desired liquid level on the tray
Types:
Y” Low weirs are frequently used in low pressure or vacuum columns.
Y” Notched (rectangular or V-shaped) weirs are commonly used for low liquid loads...
The higher the liquid level, the higher the tray pressure drop, the more liquid hold-up on the tray, which may be
undesirable if the liquid is toxic or hazardous.
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Plate Column Anatomy —
Basic Components of Tray Column
Sloped
downcomer À
= Downcomers:
The function of downcomer is to guide liquid flow from an upper tray to a lower tray.
Types:
Y” straight: is widely used as it provides good utilization of column area for downflow and has cost
and simplicity advantage
Y” Sloped: can be used if vapour-liquid disengagement is difficult (e.g. due to foaming) and also
provide a slightly larger active area for vapour-liquid contact, but is also more expensive
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Plate Column Anatomy
Basic Components of Tray Column
= Downcomers:
> A downcomer must be sufficiently large to allow liquid to flow smoothly without choking.
> Sufficient time must also be provided to allow proper vapour disengagement from the down-flowing
liquid, so that the liquid is relatively free of vapour when it enters the tray below
> Inadequate downcomer area will lead to downcomer choking, whereby liquid backs up the downcomer
into the tray above and eventually flood the column.
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Plate Column Anatomy
Basic Components of Tray Column
= Tray Manway:
> Tray manways allow maintenance workers and inspectors to travel from one tray to another.
> Manway size should be at least 16 x 20-inch.
> For multi-pass trays, one tray manway should be provided for each tray pass, as the central
downcomers restrict access from one side to the other.
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Comparison Sieve Valve Bubble Cap
Capacity Mid Highest Lowest
Pressure Drop Lower Mid Higher
Turndown Ratio Lowest [2.1] Higher [4 to 10.1] Mid
Entrainment Medium Medium Highest
Efficiency High High Lowest
Cost Cheapest 20 / 50% more than | 100/ 200% more
Sieve than Sieve
Tray vs, Packed Column for Chemical Engineering Applications
= Packed columns are more suitable for low capacity operations.
= Packed columns are particularly useful in the field of vacuum distillation.
= For separating heat sensitive materials packed columns are useful
because the liquid hold up* is low.
= When corrosion is a problem packing may be the only answer.
= Pressure drop per unit length is less in packed column.
= Total weight of packed column is less due to use of low weight and high
capacity packing.
* Liquid holdup HL, is defined as the fraction of an element of pipe which is occupied by liquid
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Packing Tower Anatomy
Introduction and Represen
ation
> Packed beds can be used in a chemical reactor, a distillation
process, or a scrubber, bu
store heat in chemical plants.
packed beds have also been used to
> The purpose of a packed bed is typically to improve contact
between two phases in a c
> The gas liquid contact in a
hemical or similar process.
packed bed column is continuous, not
stage-wise, as in a plate column.
Tray vs. Packed Column for Chemical Engineering Applic
ations
Packing Material
T
Packing
Height (Z)
L
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Packing Tower Anatomy
Packed Column Principle
v Packed towers use specially designed packing materials to
provide more surface area for maximum contact between gases
and liquids.
¥ Liquids wet the surface of the packing as they migrate down the
tower.
v Rising vapors come into contact with the wetted surface and
exchange heat.
The performance of a packed column is very dependent on the maintenance of 1
Vapour (Up-Flow)
good liquid and gas distribution throughout the packed bed. >
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Packing Tower Anatomy
Liquid travels down through feed distributors, hold-down grids,
random and structured packing, support plates, redistributors, liquid
collectors, structured grids, and finally into the bottom section.
Hot vapors move countercurrent to the downward flow of liquid.
Types of packed distillation columns:
= Random Packing
" Structured Packing
= Stacked Packing
U, Boro uno
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Packing Tower Anatomy
Packed Column Accessory
a) Shell
= The cylindrical shell of the distillation column is typically metal, carbon
steel, stainless steel, special alloy or nonferrous. .
= Columns can also be composed of glass, ceramic, plastic, or wood.
= The type of chemicals that will be used in the distillation column will
determine the design material, lining specification, wall thickness,
pressure rating, and temperature rating.
Tray vs. Packed Column for Chemical Engineering Applications
eboder Return
Han
6
Packing Tower Anatomy
Packed Column Accessory
b) 1) Random Packing
= Random packing includes discrete pieces of packing that are
randomly dumped or poured into a packed column.
Use:
= It provides a surface for good vapor-liquid contact, distillation
efficiency characteristics, and predictable pressure drop.
J =
oe, SS
Random Packing
¿Liquid
Redistributor
Hold Down Grid
Support Grid
‘ChimneyiCollector
Tray
Tray vs. Packed Column for Chemical Engineering Applications
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Packing Tower Anatomy
Random Packing
Tray vs. Packed Column for Chemical Engineering Applications engabdelrahman kamal25ägmail.com
Packing Tower Anatomy
Packed Column Accessory
b) 2) Structured packing
= Structured packing has specific geometric shapes, like a mesh.
Use:
= It works best in columns requiring high liquid loadings.
Req Random Packing
Liquid
Redistributor
— Hold Down Grid
Support Grid
L- Chimney/Collector
Tray
Tray vs. Packed Column for Chemical Engineering Applications
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Packing Tower Anatomy
Structured Packing
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Packing Tower Anatomy
Packed Column Accessory
b) 8) Stacked Packing
= Stacked packing is uniformly arranged inside a distillation column.
Use:
= Packed columns are designed for pressure drops between 0.20
and 0.60 inch of water per foot of packing medium
Random Packing
Liquid
Redistributor
Hold Down Grid
Support Grid
L- Chimney/Collector
Tray
Tray vs. Packed Column for Chemical Engineering Applications
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Packing Tower Anatomy
Packing Material
Sulzer Packing Rasching Ring
Ceramic & Metal
QR dia
ans sû 45 oe
Metal Pall Ring Intalox Saddle Metal Intalox Berl Saddle
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Packing Tower Anatomy
Packed Column Accessory
c) Packing Support
= The packing inside a distillation column is supported by packing supports.
= [tis designed to provide sufficient air-liquid passage and to prevent the packing
from migrating into the lower sections of the column.
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Bed Limiter Hold-Down Plate
Packing Tower Anatomy
Packed Column Accessory
d) Bed Limiters and Hold-Down Plates
= They are designed to keep fixed bed packing from migrating or fluidizing out of the
section.
= Hold-down plates rest on top of the packing, whereas bed limiters are attached to
the inside wall of the column.
= Hold-down plates are primarily used on carbon and ceramic packing.
= Bed limiters are used on metal or plastic packing
Tray vs. Packed Column for Chemical Engineering Applications engabdelrahman kamal25ägmail.com
Packing Tower Anatomy
Packed Column Accessory
M— Ref
e) Liquid Distribution and Redistribution “ve
= [t's so important device where it is used to disperse fluid evenly over the top
of the packing to enhance distribution of liquid through packing.
Ladder Pipe
Distributor
= Poor liquid distribution reduces vapor-liquid contact and promotes channeling
which reduces the operation efficiency of the column.
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Packing Tower Anatomy
Liquid Distributer
Orifice Type Spray Nozzle Trough Type
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Packing Tower Anatomy
Liquid Distributer
[
CASS.
Pipe Ladder Channel Distributor
Qe
Ring Distributor
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Comparison Tray Column Packed Column
Capacity Higher Lower
Diameter Larger Smaller
Cost Less Expensive More Expensive
Maintenance Easier More Difficult
Vapour Liquid Contact Less More
Side Stream Available Not Available
Corrosive Materials Not Recommended Appropriate
Side Stream
Wide range
Not recommended for low rate
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Comparison Tray Column Packed Column
Pressure Drop Higher Lower
Max Temperature Higher Lower
Toxic And Not safe Appropriate
Flammable Liquids
Fouling Liquids Appropriate Not recommended
Foaming Systems Not Recommended Appropriate
Tray vs, Packed Column for Chemical Engineering Applications engabdelrahman kamal25ägmail.com
References
= Process Technology Equipment and Systems, Charles E. Thomas 4" edition
= AICHE Resources, aiche.org
= NPTEL Website
= Chemical Engineering World Website
= Separation Processes Website
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Author Contacts
Abdelrahman Kamal
Department of Chemical Engineering and Petroleum Refining
Faculty of Petroleum and Mining Engineering, Suez University